Download Advanced x-ray crystallography by Angelo Gavezzotti (auth.), Kari Rissanen (eds.) PDF

By Angelo Gavezzotti (auth.), Kari Rissanen (eds.)

Computational experiences of Crystal constitution and Bonding, via Angelo Gavezzotti Cryo-Crystallography: Diffraction at Low Temperature and extra, by means of Piero Macchi High-Pressure Crystallography, through Malcolm I. McMahon Chemical X-Ray Photodiffraction: rules, Examples, and views, through Panče Naumov Powder Diffraction Crystallography of Molecular Solids, through Kenneth D. M. Harris

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64. 1007/128_2011_207 # Springer-Verlag Berlin Heidelberg 2011 Published online: 17 September 2011 Cryo-Crystallography: Diffraction at Low Temperature and More Piero Macchi Abstract This chapter comments on the motivations and the methods of crystallographic studies at low temperature. Cry-crystallography is a brunch of Crystallography, a science that is too often confused with a technique. On the other hand, the scientific background to study crystal phases at low temperature is here provided, together with a survey of many possible techniques that provide complementary or supplementary information.

3 Other Techniques . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Cryo-Crystallographic Studies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Crystal Structure Solution and Refinement . . . . . . . . . . . . . . . . . . . . . . 2 Accurate Electron Density . . . . . . . . . . . . . . . . . . . . . . . . . . .

2 Powder Diffraction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Other Techniques . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Cryo-Crystallographic Studies . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Crystal Structure Solution and Refinement . . . . . . . . . .

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